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Extra info for Electroanalytical Chemistry: Volume 20 (Electroanalytical Chemistry: a Series of Advances)
Example text
5. ) orientation of the crystals. This preferential orientation was maintained after their electrochemical conversion to Pb. The resulting lead crystals were then allowed to react with dissolved oxygen and chloride ions to form Pb(OH)Cl, which was later reduced back to metallic lead in a second electrochemical reaction. Even after these numerous conversions, the described preferential orientation was still detectable. Further, it is interesting to learn that this orientation was distinctly different from that of lead, which was deposited from a Pb2+ solution.
J. Girault and D. J. Schiffrin Ellipsometry: Principles and Recent Applications in Electrochemistry Shimson Gottesfeld Voltammetry at Ultramicroelectrodes R. Mark Wightman and David O. Wipf Volume 16 Voltammetry Following Nonelectrolytic Preconcentration Joseph Wang Hydrodynamic Voltammetry in Continuous-Flow Analysis Hari Gunasingham and Bernard Fleet Electrochemical Aspects of Low-Dimensional Molecular Solids Michael D. Ward Volume 17 Applications of the Quartz Crystal Microbalance to Electrochemistry Daniel A.
68] by combining VMP and in situ x-ray diffraction for the following two reactions: Bearing in mind that these electrochemical reactions are performed at room temperature, one could expect that the lead thus formed may not have the chance to crystallize, as the activation energy for the crystallization may not suffice under these conditions. The in situ study was performed with a cell as shown in Fig. 5. It was observed that reaction (IX) formed cubic lead simultaneously with the reduction of the PbO, whereas reaction (X) resulted in the formation of an x-ray amorphous phase, which only slowly crystallized to form cubic lead.